An Evaluation of Analytical and Interpretative Methodologies for the Extraction and Identification of Lipids Associated With Pottery Sherds From the Site of Sagalassos, Turkey
Bibliographic Data
| ID | 8352011 |
|---|---|
| Authors | Kerlijne Romanus (KU Leuven), Jeroen Poblome (0000-0002-7403-1921, KU Leuven), Kristin Verbeke (0000-0002-5352-7565, KU Leuven), Anja Luypaerts (KU Leuven), P Jacobs, Pierre A Jacobs (KU Leuven), D DE VOS (0000-0003-0332-0125, KU Leuven), Marc Waelkens (KU Leuven) |
| Year | 2007 |
| Volume | 49 |
| Issue | 4 |
| Pages | 729-747 |
| Publication date | 2007-11-01 |
| Peer Reviewed | Yes |
| Open Access | Yes |
| Type | ARTICLE |
| Venue | Archaeometry (JOURNAL) |
| Journal identifiers | ISSN: 0003-813X • E-ISSN: 1475-4754 |
| Publisher | Wiley (PUBLISHER • GB) |
| DOI | 10.1111/j.1475-4754.2007.00332.x |
| OpenAlex | W2018040011 |
| Language | EN |
| Citations received | 35 |
| References cited | 33 |
Three lipid analysis methods were applied to extracts of archaeological potsherds from the ancient city of Sagalassos, south‐west Turkey. In the fatty acid methyl ester fraction, obtained by selective transesterification of acylglycerols, the ratio of methyl palmitate to methyl stearate was determined. Secondly, by means of gas chromatography– combustion–isotope ratio mass spectrometry (GC–C–IRMS), stable carbon isotope ratios were measured for the same methyl esters. Finally, triglyceride composition was determined via high‐performance liquid chromatography–mass spectrometry (HPLC–MS). All three methods can be used to trace the origin of animal fat. Agreement between them is reasonable, especially in recognizing ruminant adipose fat. One sample was found to be of dairy origin using both GC–C–IRMS and HPLC–MS. The advantages of the various methods are discussed. Variations in lipid composition were observed between samples from different periods and excavated in diverse areas within the city of Sagalassos
Archaeology · Chromatography · Extraction (chemistry) · Fatty acid · Gas chromatography · Glyceride · High-performance liquid chromatography · Isotope-ratio mass spectrometry · Mass spectrometry · Pottery · Ancient Mediterranean Archaeology and History · Archaeology and ancient environmental studies · Chemistry · Cultural Heritage Materials Analysis · Environmental Chemistry · Organic Chemistry
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| Unique citing works | 35 |
|---|---|
| Citations per year | 1,94 |
| Citation span | 2008 - 2026 (19) |
| Citation velocity | current |
| Highly cited | No |
| Citation types | Neutral: 34 |