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New Synthesis and Small Angle Neutron Scattering Studies of Polyaniline Nanofibers

Bibliographic Data

ID21160226
AuthorsB Kavitha (0000-0002-6239-8128, Osmania University), K Siva Kumar (Osmania University)
Year2012
Volume16
Issue1
Pages5-7
Publication date2012-08-15
Open AccessNo
TypeARTICLE
VenueNew Materialisms (JOURNAL)
Journal identifiersISSN: 1480-2422 • E-ISSN: 2292-1168
PublisherJournal of New Materials for Electrochemical Systems (PUBLISHER)
DOI10.14447/jnmes.v16i1.30
OpenAlexW2889128390
LanguageEN

Nano structured polyaniline (PANI) is synthesized for the first time by polymerization of aniline in the presence of hydrochloric acid as a catalyst and ammoniumperoxidisulphate as an oxidant by the chemical oxidative polymerization method. The product powder was pelletized with help of hydraulic machine to study the XRD, SEM and SANS. The XRD pattern indicates semi crystalline nature of PANI with interplanar distance 4.210 Å and 3.774 Å respectively. The SEM pictures shows fiber like nature of particles. SANS experiment is used to find different parameters of these crystalline polymer particles. Dynamic light Scattering (DLS) studies are performed to find the sizes of nano structured polyaniline. The length and radius of nano size polyaniline are identified as 617.6 nm and 75.05 nm respectively

Aniline · Composite material · Conductive polymer · Dynamic light scattering · Hydrochloric acid · Nano · Nanofiber · Nanoparticle · Nanotechnology · Neutron scattering · Optics · Physics · Polyaniline · Polyaniline nanofibers · Polymer · Polymer chemistry · Polymerization · Scattering · Small-angle neutron scattering · Chemical Engineering · Chemistry · Conducting polymers and applications · Materials Science · Organic Chemistry

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