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Combined Thermal and X-Ray Diffraction Technique for Identification of Ceramicware Temper and Paste Minerals

Bibliographic Data

ID2567183
AuthorsWayne C Isphording (corresponding author)
Year1974
Volume39
Issue3
Pages477-483
Publication date1974-07-01
Open AccessYes
TypeARTICLE
VenueAmerican Antiquity (JOURNAL)
Journal identifiersISSN: 0002-7316 • E-ISSN: 2325-5064
PublisherCambridge University Press (CUP) (PUBLISHER)
DOI10.2307/279440
OpenAlexW2317227974
LanguageEN
Citations received7
References cited4

The identification of the original paste and temper minerals present in ceramicware fragments can often be useful in determining if the fragments are indigenous to the area or whether they represent tradeware. To date, it has generally been believed that no certain means existed to identify the mineral constitutents once they were destroyed in the original kiln-firing operation. A new technique is described that permits the investigator to often identify both temper and the fine-grained paste materials as well. This method involves: (1) crushing the fragment to a fine powder; (2) heating the powder in a high temperature furnace to sufficient temperatures to cause the constituent ions present to recombine to form new, high temperature minerals; and (3) X-ray diffraction analysis to identify the new minerals. In many cases, identification of the resulting high temperature minerals will clearly indicate the composition of the original clay paste and temper. Examples are shown for the clay minerals kaolinite, montmorillonite and palygorskite. Diffractograms are also presented for comparison of ceramic fragments from Mexico and Alabama that contain the above minerals as original constituents

Ceramic · Clay minerals · Composite material · Crystallography · Kaolinite · Metallurgy · Mineral · Mineralogy · Montmorillonite · Palygorskite · Powder diffraction · Building materials and conservation · Chemistry · Cultural Heritage Materials Analysis · Geology · Materials Science · Mineralogy and Gemology Studies

  • Vertisoles y cerámica indígena

    Open Access•Irina Capdepont, Gustavo Piñeiro•Revista del Museo de Antropología•2010

  • Ceramic Compositional Analysis in Archaeological Perspective

    Open Access•Ronald L Bishop, Robert L Rands et al.•Advances in archaeological method…•1982

  • Investigation of Islamic ceramics from Tell Tuneinir using X‐ray diffraction

    Open Access•Murray L Eiland, Quentin Williams•Geoarchaeology•2001

  • Maya Blue-Further Perspectives and the Possible Use of Indigo as the Colorant

    Open Access•Edwin R Littmann•American Antiquity•1982

  • Maya Blue and Palygorskite

    Open Access•Dean E Arnold•Ancient Mesoamerica•2005

  • Identifying the Mineralogy of Rock Temper in Ceramics Using X-Radiography

    Open Access•Catherine Carr, Christopher Carr et al.•American Antiquity•1995

  • Maya Blue-A New Perspective

    Open Access•Edwin R Littmann•American Antiquity•1980

  • Ceramics for the Archaeologist

    R J Gettens, Anna O Shephard•Studies in Conservation•1957

Citations per year0.15
Citation span1980 - 2010 (31)
Highly citedNo

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