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Comparison of analytical techniques for analysis of archaeological bronze

Analytical techniques for analysis of archaeological bronze

Bibliographic Data

ID8353064
AuthorsValentina Lyubomirova (0000-0002-3033-8358, Sofia University "St. Kliment Ohridski", corresponding author), R Djingova (Faculty of Chemistry and Pharmacy; University of Sofia; Blvd. James Bourchier 1 1164 Sofia Bulgaria), I Kuleff (Faculty of Chemistry and Pharmacy; University of Sofia; Blvd. James Bourchier 1 1164 Sofia Bulgaria)
Year2015
Volume57
Issue4
Pages677-686
Publication date2015-08-01
Peer ReviewedYes
Open AccessYes
TypeARTICLE
VenueArchaeometry (JOURNAL)
Journal identifiersISSN: 0003-813X • E-ISSN: 1475-4754
PublisherWiley (PUBLISHER • GB)
DOI10.1111/arcm.12138
OpenAlexW2101326207
LanguageEN
Citations received9
References cited3

While many analyses of archaeological bronzes have been reported in the literature, in practice it is very difficult to compare them. To assess the present status of the chemical analysis of bronze two ancient objects—a flat axe (arsenic bronze) and a sickle (tin bronze)—were cut into pieces weighing about 2 g each and were distributed to 11 laboratories. The participants used the following methods for analysis: INAA, ED–XRF, PIXE, TRXRF, FAAS, ICP–AES, ICP–MS, SEM–EDS, LA–ICP–MS and PGAA. The samples were analysed in at least quadruplicate. Dixon's and Iglewicz and Hoaglin's tests were used to detect outliers. The majority of methods provided comparable results, especially for macroelements, independent of the technique and standards used. The number of determined elements depended on the method and, naturally, on the concentration level. Therefore an important recommendation that can be made is to supply, with each archaeometric investigation, data from the analysis of appropriate Certified Reference Materials (CRMs) used in the study

Archaeological science · Archaeology · Bronze · Bronze Age · Certified reference materials · Geography · Statistics · Archaeology and ancient environmental studies · Cultural Heritage Materials Analysis · Mathematics · X-ray Spectroscopy and Fluorescence Analysis

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Unique citing works9
Citations per year0,9
Citation span2016 - 2026 (11)
Citation velocitycurrent
Highly citedNo
Citation typesNeutral: 8

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