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High Precision 14 C Analysis in Small Seawater Samples

Bibliographic Data

ID9244273
AuthorsNúria Casacuberta (0000-0001-7316-1655), Maxi Castrillejo (0000-0001-5149-2218), Anne-Marie Wefing, Silvia Bollhalder, Lukas Wacker (0000-0002-8215-2678)
Year2020
Volume62
Issue1
Pages13-24
Publication date2020-02-01
Peer ReviewedYes
Open AccessYes
TypeARTICLE
VenueRadiocarbon (JOURNAL)
Journal identifiersISSN: 0033-8222 • E-ISSN: 1945-5755
PublisherCambridge University Press (CUP) (PUBLISHER)
DOI10.1017/rdc.2019.87
OpenAlexW2969931555
LanguageEN
Citations received5
References cited20

A new method to extract CO 2 in seawater samples for the determination of F 14 C has been developed in the Laboratory of Ion Beam Physics at ETH Zurich. The setup consists of an automated sampler designed to extract dissolved inorganic carbon (DIC) from 7 samples in a row, by flushing the seawater with He gas to extract CO 2 . The fully automated method is controlled via a LabVIEW program that runs through all consecutive steps: catalyst preconditioning, CO 2 extraction, CO 2 trapping, thermal CO 2 release from the trap into the reactor and finally the graphitization reaction which is performed simultaneously in the 7 reactors. The method was optimized by introducing a Cu-Ag furnace that was placed between the water and zeolite traps, which resulted in a better and faster graphitization performance ( 14 C) as water mass tracer

Carbon fibers · Chromatography · Mass spectrometry · Mineralogy · Nuclear physics · Physics · Seawater · TRACER · Chemistry · Environmental Science · Isotope Analysis in Ecology · Materials Science · Methane Hydrates and Related Phenomena · Nuclear Physics and Applications · Environmental Chemistry · Geology · Oceanography

  • Radiocarbon measurements of dissolved inorganic carbon (DIC) in sediment porewater and seawater at AWI Micadas

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  • A revolutionary graphitisation system

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Unique citing works5
Citations per year1
Citation span2021 - 2026 (6)
Citation velocitycurrent
Highly citedNo
Citation typesNeutral: 5

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