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Direct Absorption Method and Liquid Scintillation Counting for Radiocarbon Measurements in Organic Carbon from Sediments

Bibliographic Data

ID9245638
AuthorsIonut Făurescu (0000-0001-9811-5751), Carmen Varlam (0000-0003-3325-822X), Ioan Stefanescu, Stela Cuna, Irina Vagner (0000-0001-7164-4215), Denisa Făurescu (0000-0002-5585-4690), Diana Bogdan
Year2010
Volume52
Issue2
Pages794-799
Publication date2010-01-01
Open AccessYes
TypeARTICLE
VenueRadiocarbon (JOURNAL)
Journal identifiersISSN: 0033-8222 • E-ISSN: 1945-5755
PublisherCambridge University Press (CUP) (PUBLISHER)
DOI10.1017/s003382220004580x
OpenAlexW1895765583
LanguageEN
References cited2

In this paper, we investigate a procedure for radiocarbon determination in forest soil and slurry from lake sediments. The total carbon in these samples can be both inorganic and organic. Inorganic carbon can be analyzed in a straightforward manner using the direct absorption method by sample acidification and CO 2 capture. For organic carbon, we investigate a hybrid method using the wet-oxidation of organic carbon followed by direct absorption. To evaluate the wet-oxidation processes with potassium dichromate (K 2 Cr 2 O 7 ) and potassium permanganate (KMnO 4 ), we performed several experiments using different quantities of soil and sediments in order to establish the quantity of CO 2 for each type of sample. The 2 methods offer comparable results for 14 C-specific activity (about 0.234 ± 0.024 Bq/g C), values that are expected for these kinds of samples. We also investigated the possibility of isotopic fractionation occurring during CO 2 production from raw material by measuring δ 13 C levels from samples and obtained CO 2

Carbon fibers · Carbon-14 · Chromatography · Fractionation · Liquid scintillation counting · Mineralogy · Organic matter · Potassium dichromate · Potassium permanganate · Radiocarbon dating · Radiochemistry · Slurry · Soil test · Soil water · Total organic carbon · Wet oxidation · Atmospheric and Environmental Gas Dynamics · Chemistry · Environmental Science · Geology and Paleoclimatology Research · Isotope Analysis in Ecology · Materials Science · Environmental Chemistry · Environmental Engineering · Geology · Inorganic Chemistry · Soil Science

  • Applying the Direct Absorption Method and LSC for 14 C Concentration Measurement in Aqueous Samples

    Open Access•Carmen Varlam, Ioan Stefanescu et al.•Radiocarbon•2007

Highly citedNo

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